Photonic Materials Technology Section (PMTS)
RRCAT_Indore Photonic Materials Technology Section (PMTS)
RRCAT_Indore Photonic & Detector Materials Laboratory (PDML)

Device relevant characterization of single crystals using optical and X-ray techniques

X-ray diffraction topographic imaging of defects in crystals

X-ray diffraction topography is used for characterizing defects state of the crystal. In particular, the following defects can be visualized:

Line defects:Dislocations
Planar defects :Growth striations, growth sector boundaries
Volume defects:Inclusions, bubbles, precipitates
Mechanical defects:Cracks, scratches, indentations


Origin of topographic contrast:

It is based on Bragg’s law, 2dhkl sin⁡θ=nλ. Defects result in lattice misorientations (δθ), which is maximum in the vicinity of the defect and zero sufficiently away from it. These misoriented lattice planes do not satisfy the Braggs Law which leads to low diffracted intensities and hence image with varying degree of contrast is imaged.

X-ray topogrpahic images of crystalline sample [Cryst Eng Comm 15 (2013) 9955; RRCAT Newsletter 26 (2) (2013) 26; Opt. Mater. 46 (2015) 329]
X-ray topogrpahic images of crystalline sample [Cryst Eng Comm 15 (2013) 9955; RRCAT Newsletter 26 (2) (2013) 26; Opt. Mater. 46 (2015) 329]


The crystalline quality and optical homogeneity of the grown crystals was assessed using conoscopy, birefringence interferometry and high resolution XRD technique. [Cryst. Res. Technol., 43 (4) (2008) 438-442; Cryst. Growth Des., 8 (12) (2008) 4424-4427; Cryst. Res. Technol., 44 (3) (2009) 305-308; Physica-B 404 (20) (2009) 3507-3509; Cryst. Res. Technol. 44 (12) (2009) 1303-1307]
The crystalline quality and optical homogeneity of the grown crystals was assessed using conoscopy, birefringence interferometry and high resolution XRD technique. [Cryst. Res. Technol., 43 (4) (2008) 438-442; Cryst. Growth Des., 8 (12) (2008) 4424-4427; Cryst. Res. Technol., 44 (3) (2009) 305-308; Physica-B 404 (20) (2009) 3507-3509; Cryst. Res. Technol. 44 (12) (2009) 1303-1307]

Two-wave coupling studies for investigating photorefractive properties of photonic single crystals and polymer composites

Two-wave coupling set up for optical data storage properties of photorefractive crystals
Two-wave coupling set up for optical data storage properties of photorefractive crystals

Diffraction efficiency of Fe:LN as a function of annealing and proton exchange processes [Physica B 404 (2009) 3507-3509]
Diffraction efficiency of Fe:LN as a function of annealing and proton exchange processes [Physica B 404 (2009) 3507-3509]

Optical data storage properties of  Fe:LN and FeMn:LN  congruent lithium niobate crystals [Proc. PHOTONICS-2008, IIT Delhi; Proc. NLS-19 (2010), RRCAT Indore]
Optical data storage properties of Fe:LN and FeMn:LN congruent lithium niobate crystals [Proc. PHOTONICS-2008, IIT Delhi; Proc. NLS-19 (2010), RRCAT Indore]

Two wave coupling set up for quantifying photorefractive properties of polymer composites [Proc. NLS-28 (2020), VIT Chennai]
Two wave coupling set up for quantifying photorefractive properties of polymer composites [Proc. NLS-28 (2020), VIT Chennai]
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